Upload 9 files

msp_paragraph_level_no_spans_test.json

@@ -0,0 +1,1544 @@
+[
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1002/ente.201300102\nUltrathin Surface Modification by Atomic Layer Deposition on High Voltage Cathode LiNi 0.5 Mn 1.5 O 4 for Lithium Ion Batteries\n\n\nLiNi0.5Mn1.5O4 particles were synthesized through solid-state reactions. Nickel acetate [Ni(Ac)2[?]4 H2O] and manganese acetate [Mn(Ac)2[?]4 H2O] were mixed at a molar ratio of Ni/Mn=1:3 and milled in a mortar. After heating at 500 degC for 5 h, lithium acetate (LiAc[?]2 H2O) was added to the mixture at a molar ratio of Li/Ni/Mn=2.1:1:3 (5 % excess Li source was added to balance for the volatilized Li during calcination), and the mixture was heated to 500 degC for 5 h once more. Then the mixture was milled and sintered at 950 degC for 10 h followed by annealing at 700 degC for 10 h.\n\n\n\n",
+        "measurement_extractions": [
+            {
+                "docId": "101002ente201300102",
+                "quantity": "500 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "heating"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "5 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "heating"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "5 %",
+                "unit": "%",
+                "measured_entity": "Li source",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "500 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "5 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "2.1:1:3",
+                "unit": null,
+                "measured_entity": "Li/Ni/Mn",
+                "measured_property": "molar ratio"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "1:3",
+                "unit": null,
+                "measured_entity": "Ni/Mn",
+                "measured_property": "molar ratio"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "950 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "sintered"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "milled and sintered"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "700 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "annealing"
+            },
+            {
+                "docId": "101002ente201300102",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "annealing"
+            }
+        ],
+        "split": "test",
+        "docId": "101002ente201300102",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "LiMnPO4 plates were synthesized by a hydrothermal method. In a typical synthesis procedure, 14 mmol Na2S*9H2O, 40 mmol Li2SO4*H2O, 20 mmol MnSO4*H2O and 20 mmol NH4H2PO4 were added in sequence in a 40 mL Teflon liner with 30 mL distilled water under vigorous stirring for 30 min, and the Teflon liner was then placed in a stainless steel autoclave. The sealed tank was put into an oven and maintained at 200 degC for 10 h. After the hydrothermal reaction, the autoclave was cooled to room temperature and the resulted precipitate was filtered, washed and finally dried in air at 60 degC overnight.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "200 degC",
+                "unit": "degC",
+                "measured_entity": "sealed tank",
+                "measured_property": "maintained"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "sealed tank",
+                "measured_property": "maintained"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "precipitate",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "14 mmol",
+                "unit": "mmol",
+                "measured_entity": "Na2S*9H2O",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "40 mmol",
+                "unit": "mmol",
+                "measured_entity": "Li2SO4*H2O",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "20 mmol",
+                "unit": "mmol",
+                "measured_entity": "MnSO4*H2O",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "20 mmol",
+                "unit": "mmol",
+                "measured_entity": "NH4H2PO4",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "40 mL",
+                "unit": "mL",
+                "measured_entity": "Teflon liner",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "30 mL",
+                "unit": "mL",
+                "measured_entity": "distilled water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201209106",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "14 mmol Na2S*9H2O, 40 mmol Li2SO4*H2O, 20 mmol MnSO4*H2O and 20 mmol NH4H2PO4 were added in sequence in a 40 mL Teflon liner with 30 mL distilled water",
+                "measured_property": "stirring"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jelectacta201209106",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.electacta.2014.04.056\nEffects of highly crumpled graphene nanosheets on the electrochemical performances of pseudocapacitor electrode materials\n\n All chemicals were of analytical grade and used without further purification. In a typical synthesis process, 5 mg GS and 0.3 g NiCl2*6H2O were dispersed in 20 ml distilled water and subjected to ultrasonic vibration to form a homogeneous suspension, respectively. The two former suspensions were homogeneously mixed with each other and subjected to ultrasonic vibration for a while, and then freeze drying (named as M1). The 1.03 g NaH2PO2*H2O was grinded in a mortar and mixed with M1. Then, the mixture was calcined at 500 degC for 1 h with 2 degC/min heating rate and cooled to room temperature under a flow of Ar (99.999%). The solid obtained was washed thoroughly with distilled water and absolute ethyl alcohol to remove the by-products. After that, the wet products were dried at 80 degC for 12 h in a vacuum oven.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "5 mg",
+                "unit": "mg",
+                "measured_entity": "GS",
+                "measured_property": "dispersed"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "0.3 g",
+                "unit": "g",
+                "measured_entity": "dispersed",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "20 ml",
+                "unit": "ml",
+                "measured_entity": "distilled water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "1.03 g",
+                "unit": "g",
+                "measured_entity": "NaH2PO2*H2O",
+                "measured_property": "grinded"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "500 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "1 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "2 degC/min",
+                "unit": "degC/min",
+                "measured_entity": "mixture",
+                "measured_property": "heating rate"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "99.999%",
+                "unit": "%",
+                "measured_entity": "Ar",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "wet products",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jelectacta201404056",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "wet products",
+                "measured_property": "dried"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jelectacta201404056",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.electacta.2014.08.103\nFacile synthesis of heterogeneous Ni-Si@C nanocomposites as high-performance anodes for Li-ion batteries\n\nBefore the electrical pulse process with Ni wire, Si nanoparticles (0.2, 0.6, and 0.8 g) were first dispersed in 700 mL of OA, and the Si nanoparticles-dispersed suspension was sonicated for 1 h. Then, the electrical wire explosion (NTi-mini P, Nano Tech, Korea) was conducted at a feeding distance of 40 mm and a charge voltage of 320 V in the Si nanoparticles-dispersed suspension. After completing the electrical pulse treatment with Ni wire, the obtained brownish Ni-Si nanocolloidal suspension was sonicated and filtered through a nylon membrane (Durapore, 0.22 mm, Millipore) several times and subsequently dried at 120 degC for 10 h. Finally, the carbon-coated Ni-Si nanocomposites were obtained via carbonization process (heat-treatment) carried out at 500 degC for 5 h in an Ar atmosphere.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "0.2, 0.6, and 0.8 g",
+                "unit": "g",
+                "measured_entity": "Si nanoparticles",
+                "measured_property": "dispersed"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "700 mL",
+                "unit": "mL",
+                "measured_entity": "OA",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "1 h",
+                "unit": "h",
+                "measured_entity": "Si nanoparticles-dispersed suspension",
+                "measured_property": "sonicated"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "40 mm",
+                "unit": "mm",
+                "measured_entity": "electrical wire explosion",
+                "measured_property": "feeding distance"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "320 V",
+                "unit": "V",
+                "measured_entity": "electrical wire explosion",
+                "measured_property": "charge voltage"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "120 degC",
+                "unit": "degC",
+                "measured_entity": "brownish Ni-Si nanocolloidal suspension",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "brownish Ni-Si nanocolloidal suspension",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "0.22 mm",
+                "unit": "mm",
+                "measured_entity": "nylon membrane (Durapore",
+                "measured_property": "Millipore"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "500 degC",
+                "unit": "degC",
+                "measured_entity": "carbon-coated Ni-Si nanocomposites",
+                "measured_property": "carbonization process (heat-treatment)"
+            },
+            {
+                "docId": "101016jelectacta201408103",
+                "quantity": "5 h",
+                "unit": "h",
+                "measured_entity": "carbon-coated Ni-Si nanocomposites",
+                "measured_property": "carbonization process (heat-treatment)"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jelectacta201408103",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.electacta.2014.12.157\nSynthesis and electrochemical performance of ZnCo2O4 for lithium-ion battery application\n\n\nAll of the chemicals in our synthesis were analytical grade and were used without further purification. In a typical procedure, zinc acetate dihydrate and cobalt (II) acetate tetrahydrate with a Zn/Co molar ratio of 1:2 were added to a ball mill. Citric acid with a 120% mole fraction relative to the Zn and Co was then added into the ball mill. After adding a suitable volume of water, the ball mill was run for 4 h at 500 rpm to obtain the precursor. Then, the resultant mixture was dried at 80 degC in air, and the wine red precursor powder was collected and heat-treated in a muffle furnace at 400 degC and 500 degC, with the products designated as 400-ZCO and 500-ZCO, respectively.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "120%",
+                "unit": "%",
+                "measured_entity": "Citric acid",
+                "measured_property": "mole fraction relative to the Zn and Co"
+            },
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "1:2",
+                "unit": null,
+                "measured_entity": "zinc acetate dihydrate and cobalt (II) acetate tetrahydrate",
+                "measured_property": "molar ratio"
+            },
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "400 degC and 500 degC",
+                "unit": "degC",
+                "measured_entity": "wine red precursor powder",
+                "measured_property": "heat-treated"
+            },
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "ball mill",
+                "measured_property": "run"
+            },
+            {
+                "docId": "101016jelectacta201412157",
+                "quantity": "500 rpm",
+                "unit": "rpm",
+                "measured_entity": "ball mill",
+                "measured_property": "run"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jelectacta201412157",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.energy.2014.08.058\nHierarchical 3D micro-/nano-V2O5 (vanadium pentoxide) spheres as cathode materials for high-energy and high-power lithium ion-batteries\n\nHierarchical 3D micro-/nano-V2O5 spheres were prepared via a facile low temperature hydrothermal method. Typically, NH4VO3 (ammonium metavanadate) solution, HCl, and poly (sodium 4-styrenesulfonate) (PSS, 2 mL) were well mixed in DI (deionized) water. The pH of the mixed solution was adjusted to be less than 2.7 so as to assist the growth of V2O5[58]. The resultant solution was transferred into a 100 mL Teflon-lined autoclave and heated to 180 degC for 24 h in an electrical oven. After cooling down naturally to room temperature, the precipitates were washed with DI water and ethanol alternatively for several times to remove residual starting materials before further characterization and electrochemical testing.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jenergy201408058",
+                "quantity": "less than 2.7",
+                "unit": null,
+                "measured_entity": "mixed solution",
+                "measured_property": "adjusted"
+            },
+            {
+                "docId": "101016jenergy201408058",
+                "quantity": "2 mL",
+                "unit": "mL",
+                "measured_entity": "poly (sodium 4-styrenesulfonate)",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101016jenergy201408058",
+                "quantity": "100 mL",
+                "unit": "mL",
+                "measured_entity": "Teflon-lined autoclave",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jenergy201408058",
+                "quantity": "180 degC",
+                "unit": "degC",
+                "measured_entity": "resultant solution",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jenergy201408058",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "resultant solution",
+                "measured_property": "heated"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jenergy201408058",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "Tailoring of phase composition and morphology of TiO2-based electrode materials for lithium-ion batteries\n\nThe mixed titania phases were synthesized via hydrothermal treatment in alkaline environment based on procedure by Yoshida et al. As starting material TiO2 from Umicore was used which was mixed with NaOH in distilled water. Throughout stirring a homogeneous solution was obtained which was transferred into a Teflon lined autoclave and kept at 150 degC for 72 h. After cooling naturally to ambient temperature the white, sorbet-like product was washed in distilled water to eliminate remaining NaOH before washing in 0.1 M HCl at pH <= 2. In a final washing step the solution was brought to neutrality. Subsequently the product was dried at [?]100 degC, ground and sieved to a 50 \u03bcm mesh. In a final preparation step the white powder samples were heat treated in air at 450 degC for 4 h in air.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "150 degC",
+                "unit": "degC",
+                "measured_entity": "homogeneous solution",
+                "measured_property": "kept"
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "72 h",
+                "unit": "h",
+                "measured_entity": "homogeneous solution",
+                "measured_property": "kept"
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "0.1 M",
+                "unit": "M",
+                "measured_entity": "HCl",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "<= 2",
+                "unit": null,
+                "measured_entity": "0.1 M HCl",
+                "measured_property": "pH"
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "100 degC",
+                "unit": "degC",
+                "measured_entity": "product",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "50 \u03bcm",
+                "unit": "\u03bcm",
+                "measured_entity": "mesh",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "450 degC",
+                "unit": "degC",
+                "measured_entity": "white powder samples",
+                "measured_property": "heat treated"
+            },
+            {
+                "docId": "101016jjpowsour201212058",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "white powder samples",
+                "measured_property": "heat treated"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jjpowsour201212058",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "j.jpowsour.2013.10.120\nFabrication and performance of BaCe0.8Y0.2O3-\u03b4-BaZr0.8Y0.2O3-\u03b4 bilayer electrolyte for anode-supported solid oxide fuel cells\n\nBCY and BZCY powders were fabricated using a citric acid-nitrate gel combustion process [15]. First, BaCO3, Ce(NO3)4*4H2O, Zr(NO3)4 *5H2O and Y(NO3)3*6H2O was added to a solution of HNO3. After the solution became clear, citric acid was added in a 1:1.5 metal ions:citric acid molar ratio. The solution was continuously stirred and heated at 70 degC until a gel formed. The gel was then heated on a hot plate and combusted to form powder precursors, which were then calcined at 1000 degC for 3 h to obtain a pure, crystalline BCY and BZCY phase. NiO (basic nickel carbonate decomposed at 600 degC) and BZCY were mixed by ball milling in ethanol for 24 h in a weight ratio of 60/40 with 10 wt.% of starch as pore formers. The mixture was dried in an oven at 60 degC and prepared as anode supporting substrates.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "70 degC",
+                "unit": "degC",
+                "measured_entity": "solution",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "1000 degC",
+                "unit": "degC",
+                "measured_entity": "powder precursors",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "3 h",
+                "unit": "h",
+                "measured_entity": "powder precursors",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "1:1.5",
+                "unit": null,
+                "measured_entity": "metal ions:citric acid",
+                "measured_property": "molar ratio"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "NiO (basic nickel carbonate decomposed at 600 degC) and BZCY",
+                "measured_property": "mixed by ball milling in ethanol"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "60/40",
+                "unit": null,
+                "measured_entity": "NiO (basic nickel carbonate decomposed at 600 degC) and BZCY",
+                "measured_property": "weight ratio"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "10 wt.%",
+                "unit": "wt.%",
+                "measured_entity": "starch",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "600 degC",
+                "unit": "degC",
+                "measured_entity": "basic nickel carbonate",
+                "measured_property": "decomposed"
+            },
+            {
+                "docId": "101016jjpowsour201310120",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "dried"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jjpowsour201310120",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "(001) Si wafers were etched by mixed solution of 0.4 M AgNO3 and HF for 30 min. After the etching process, the by-products (Ag nanostructures) were removed by nitric acid, leaving the nanowire bundles (Fig. 1(a)). The samples were cleaned by deionized water and dilute HF is used to remove the surface oxide. Then different amount of hydrazine monohydrate (98%) was controlled and infiltrated through the as-formed nanowires (Fig. 1(b)). A solution of mixing BiCl3 (0.2 M) in nitric acid and H6TeO6 (0.15 M) in deionized water was prepared, followed by the addition of thioglycolic acid for the formation of the mixed complex at room temperature. Then the solution temperature was raised to 90 degC and Bi2Te3 nanoparticles were synthesized when dipping the hydrazine-coated samples in the as-prepared solution for the reduction of the Bi2Te3 (Fig. 1(c)). The as-synthesized samples were then washed with excess acetone and dried by N2 blow.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "90 degC",
+                "unit": "degC",
+                "measured_entity": "solution",
+                "measured_property": "temperature"
+            },
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "0.2 M",
+                "unit": "M",
+                "measured_entity": "BiCl3",
+                "measured_property": "mixing"
+            },
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "0.15 M",
+                "unit": "M",
+                "measured_entity": "H6TeO6",
+                "measured_property": "mixing"
+            },
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "0.4 M",
+                "unit": "M",
+                "measured_entity": "mixed solution",
+                "measured_property": "AgNO3 and HF"
+            },
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "Si wafers",
+                "measured_property": "etched"
+            },
+            {
+                "docId": "101016jnanoen201411053",
+                "quantity": "98%",
+                "unit": "%",
+                "measured_entity": "hydrazine monohydrate",
+                "measured_property": null
+            }
+        ],
+        "split": "test",
+        "docId": "101016jnanoen201411053",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.nanoen.2016.05.050\nNaV3(PO4)3/C nanocomposite as novel anode material for Na-ion batteries with high stability\n\nNaV3(PO4)3/C was synthesized by a sol-gel process and followed by carbon thermal reduction synthesis. Typically, 6 mmol NH4VO3 were added to 70 mL deionized water maintaining at 80 degC with continuous stirring to obtain a clear yellow solution, and then 6 mmol NH4H2PO4, 2 mmol Na2CO3 and 4 mmol citric acid were added. The gel was dried in an oven at 150 degC for 4 h, and heat-treated at 400 degC for 5 h under nitrogen atmosphere to remove CO2, H2O, and NH3. Afterward, the powder was grounded and annealed at 900 degC under H2/Ar flow (10% H2) for 12 h to produce the final compound.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "6 mmol",
+                "unit": "mmol",
+                "measured_entity": "NH4VO3",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "70 mL",
+                "unit": "mL",
+                "measured_entity": "deionized water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "6 mmol NH4VO3 were added to 70 mL deionized water",
+                "measured_property": "maintaining"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "6 mmol",
+                "unit": "mmol",
+                "measured_entity": "NH4H2PO4",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "2 mmol",
+                "unit": "mmol",
+                "measured_entity": "Na2CO3",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "4 mmol",
+                "unit": "mmol",
+                "measured_entity": "citric acid",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "900 degC",
+                "unit": "degC",
+                "measured_entity": "powder",
+                "measured_property": "annealed"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "10%",
+                "unit": "%",
+                "measured_entity": "H2",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "H2/Ar",
+                "measured_property": "annealed"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "150 degC",
+                "unit": "degC",
+                "measured_entity": "dried",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "gel",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "400 degC",
+                "unit": "degC",
+                "measured_entity": "gel",
+                "measured_property": "heat-treated"
+            },
+            {
+                "docId": "101016jnanoen201605050",
+                "quantity": "5 h",
+                "unit": "h",
+                "measured_entity": "gel",
+                "measured_property": "heat-treated"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jnanoen201605050",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.poly.2011.06.009\nPhotoinduced electron transfer in pentacoordinated complex of zinc tetraphenylporphyrin and isoquinoline N-oxide. Crystal structure, spectroscopy and DFT studies\nTetraphenylporphine (TPP) was prepared from pyrrole and benzaldehyde in boiling propionic acid [22]. Pyrrole was obtained by the known method [23] using the thermal decomposition of diammonium salt of mucic acid which was prepared from mucic acid and NH4OH. Mucic acid was synthesized by galactose oxidation with HNO3 upon heating [24]. \nZn-tetraphenylporphine (Zn-TPP) was synthesized according to known procedure [25] with some changes. Tetraphenylporphine (TPP) in CHCl3 was kept over PbO2 during 2 days to remove admixture of tetraphenylchlorine (2-10% of which can be formed at TPP synthesis) and a radical of unknown structure [26]. A mixture of 0.5 g (0.813 mmol) TPP, 0.25 g (1.14 mmol, 1.4-fold excess) of (CH3COO)2Zn*2H2O, 50 mL of chloroform and 250 mL of glacial acetic acid was boiled for 1 h (using of 7-fold excess of (CH3COO)2Zn leads to the final substance almost without the initial TPP). The resultant dark blue crystals of Zn-TPP were washed with acetic acid. Then the substance was chromatographed on an alumina column with chloroform. TLC was used (Silufol, chloroform-hexane 2:1) for Zn-TPP purity determination. To 34 mg (0.05 mM) of Zn-TPP dissolved in 15 mL of acetone, 1 mL of an acetone solution of isoquinoline N-oxide (7.3 mg, 0.05 mM) was added. The red-violet crystals appeared in 30 min, which were washed with acetone (1 mL, 2 times) and air dried.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "0.5 g",
+                "unit": "g",
+                "measured_entity": "TPP",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "0.813 mmol",
+                "unit": "mmol",
+                "measured_entity": "TPP",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "0.25 g",
+                "unit": "g",
+                "measured_entity": "(CH3COO)2Zn*2H2O",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "1.14 mmol",
+                "unit": "mmol",
+                "measured_entity": "(CH3COO)2Zn*2H2O",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "50 mL",
+                "unit": "mL",
+                "measured_entity": "chloroform",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "250 mL",
+                "unit": "mL",
+                "measured_entity": "glacial acetic acid",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "1 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "boiled"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "34 mg",
+                "unit": "mg",
+                "measured_entity": "Zn-TPP",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "0.05 mM",
+                "unit": "mM",
+                "measured_entity": "Zn-TPP",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "15 mL",
+                "unit": "mL",
+                "measured_entity": "acetone",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "1 mL",
+                "unit": "mL",
+                "measured_entity": "acetone solution",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "7.3 mg",
+                "unit": "mg",
+                "measured_entity": "isoquinoline N-oxide",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "0.05 mM",
+                "unit": "mM",
+                "measured_entity": "isoquinoline N-oxide",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "red-violet crystals",
+                "measured_property": "appeared"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "1 mL",
+                "unit": "mL",
+                "measured_entity": "acetone",
+                "measured_property": "washed"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "2 times",
+                "unit": "times",
+                "measured_entity": "acetone",
+                "measured_property": "washed"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "2 days",
+                "unit": "days",
+                "measured_entity": "Tetraphenylporphine (TPP) in CHCl3",
+                "measured_property": "kept over PbO2"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "2-10%",
+                "unit": "%",
+                "measured_entity": "admixture",
+                "measured_property": "tetraphenylchlorine"
+            },
+            {
+                "docId": "101016jpoly201106009",
+                "quantity": "2:1",
+                "unit": null,
+                "measured_entity": "TLC",
+                "measured_property": "Silufol, chloroform-hexane"
+            }
+        ],
+        "split": "test",
+        "docId": "101016jpoly201106009",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1038/srep43506\nMultifunctional Nanographene Oxide for Targeted Gene-Mediated Thermochemotherapy of Drug-resistant Tumour\nGraphite powder was purchased from Acros. KMnO4 (AR), NaNO3 (AR), linear chain PEG amine (5000), branched polyethylenimine 10000 (BPEI 10000), folic acid, EDC and NHS, were purchased from Sigma-Aldrich. Doxorubicin was purchased from Sangon Biotech (Shanghai, China). Modified RPMI-1640 Medium was purchased from HyClone. Fetal bovine serum (FBS), penicillin-streptomycin, and trypsin were obtained from Gibco. Propidium iodide, LysoTracker, MitoTracker and Hoechst were purchased from Molecular Probes (USA). The Cell Counting Kit-8 (CCK-8) and Calcein AM were purchased from Dojindo (Japan). The \u03b2-actin antibody was purchased from GeneTex (USA). The dialysis bags and ultrafiltration tubes (molecular weight cutoff: 10-kDa and 30-kDa) were purchased from Millipore. The P-gp siRNA, the scrambled siRNA and FAM-labelled siRNA were supplied by GenePharma (Shanghai, China). \nPPG was prepared based on our previously reported methods27,28. Briefly, to strongly bind negatively charged siRNA via electrostatic interactions, we used the high molecular weight branched polyethylenimine (10000) instead of low molecular weight branched polyethylenimine (1800) to modify PG via using cross-linking reagents EDC and NHS. Firstly, 40 mg EDC and 40 mg NHS were mixed in 4 mL FA (0.5 mg/mL, DMSO) solution and magnetically stirred at room temperature for 15 min, after activation, 4 ml PPG (1.0 mg/mL) solution was added in the solution to react at room temperature for 24 h. Finally, excess FA was removed by dialyzing against double distilled water (DD) for 24 h (molecular weight cutoff: 10-kDa). PPG-FA was obtained in an amount equal to NGO-PEG (0.5 mg/mL). \nPreparation of PPG-FA/Dox. Dox was loaded onto PPG-FA via the following method. Briefly, 500 \u03bcL PPG-FA (0.5 mg/mL) and 500 \u03bcL Dox (1 mg/mL) were mixed in a 5 mL PBS solution and magnetically stirred at room temperature for 12 h. Then, excess Dox was removed by dialyzing the entire system against DD water until the filtrate was free of red colour. \nPreparation of PPG-FA/siRNA: The P-gp siRNA, scrambled siRNA and FAM-labelled siRNA were respectively dissolved in DEPC-treated water to achieve 0.1 mg/mL solution. The PPG-FA was blend with different siRNA solution at a weight ratio of 4:1 (NGO: siRNA), and incubated at room temperature for 30 min. It allows the electrostatic adsorption between negatively charged siRNA and positively charged PPG-FA. For preparation of PPG-FA/Dox/siRNA, the procedures were the same as that for PPG-FA/siRNA except using PPG-FA/Dox dispersed in DEPC-treated water.",
+        "measurement_extractions": [
+            {
+                "docId": "101038srep43506",
+                "quantity": "40 mg",
+                "unit": "mg",
+                "measured_entity": "EDC",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "40 mg",
+                "unit": "mg",
+                "measured_entity": "NHS",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "4 mL",
+                "unit": "mL",
+                "measured_entity": "FA (0.5 mg/mL, DMSO) solution",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "0.5 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "solution",
+                "measured_property": "FA"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "15 min",
+                "unit": "min",
+                "measured_entity": "40 mg EDC and 40 mg NHS were mixed in 4 mL FA (0.5 mg/mL, DMSO) solution",
+                "measured_property": "stirred"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "4 ml",
+                "unit": "ml",
+                "measured_entity": "PPG (1.0 mg/mL) solution",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "1.0 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "solution",
+                "measured_property": "PPG"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "solution",
+                "measured_property": "react"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "0.1 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "solution",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "4:1",
+                "unit": null,
+                "measured_entity": "NGO: siRNA",
+                "measured_property": "weight ratio"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "PPG-FA was blend with different siRNA solution at a weight ratio of 4:1 (NGO: siRNA)",
+                "measured_property": "incubated"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "10000",
+                "unit": null,
+                "measured_entity": "branched polyethylenimine",
+                "measured_property": "high molecular weight"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "1800",
+                "unit": null,
+                "measured_entity": "branched polyethylenimine",
+                "measured_property": "low molecular weight"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "excess FA",
+                "measured_property": "removed by dialyzing against double distilled water (DD)"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "10-kDa",
+                "unit": "kDa",
+                "measured_entity": "dialyzing",
+                "measured_property": "molecular weight cutoff"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "0.5 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "NGO-PEG",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "500 \u03bcL",
+                "unit": "\u03bcL",
+                "measured_entity": "PPG-FA",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "0.5 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "PPG-FA",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "500 \u03bcL",
+                "unit": "\u03bcL",
+                "measured_entity": "Dox",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "5 mL",
+                "unit": "mL",
+                "measured_entity": "PBS solution",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "500 \u03bcL PPG-FA (0.5 mg/mL) and 500 \u03bcL Dox (1 mg/mL) were mixed in a 5 mL PBS solution",
+                "measured_property": "magnetically stirred"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "1 mg/mL",
+                "unit": "mg/mL",
+                "measured_entity": "Dox",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "10-kDa",
+                "unit": "kDa",
+                "measured_entity": "dialysis bags",
+                "measured_property": "molecular weight cutoff"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "30-kDa",
+                "unit": "kDa",
+                "measured_entity": "ultrafiltration tubes",
+                "measured_property": "molecular weight cutoff"
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "5000",
+                "unit": null,
+                "measured_entity": "linear chain PEG amine",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "10000",
+                "unit": null,
+                "measured_entity": "branched polyethylenimine",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep43506",
+                "quantity": "10000",
+                "unit": null,
+                "measured_entity": "BPEI",
+                "measured_property": null
+            }
+        ],
+        "split": "test",
+        "docId": "101038srep43506",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1039/c3gc41362d\nInsights into the stability of gold nanoparticles supported on metal oxides for the base-free oxidation of glucose to gluconic acid\nAu was deposited on the metal oxides by the deposition-precipitation method.30 A solution of HAuCl4*3H2O (175 mg) in deionized water (80 mL) was brought to pH 10 by adding a NaOH solution (0.2 M). This solution was mixed with a suspension containing the metal oxide (2 g) in deionized water (25 mL). After stirring for 18 h, the suspension was filtered and washed with an excess amount of deionized water until no more chlorine could be detected by the AgCl test. The supported Au catalyst was dried overnight at 80 degC and then reduced for 4 h at 225 degC in 5% H2 in N2 (100 mL min-1). \nThe Au/AC catalyst was prepared according to the procedure reported by Biella et al.12 A solution of HAuCl4*3H2O (1 L, 100 \u03bcg mL-1) was mixed with 2.5 g of a 2 wt% solution of poly(vinyl alcohol) (PVA, MW ~ 10000). To this solution, 0.1 M NaBH4 solution (20 mL) was added dropwise, leading to the formation of metallic Au NPs. The PVA stabilized Au NPs were then immobilized on activated carbon (Darco(r), 100 mesh) by adding 2 g of the support. The as-synthesized Au/AC catalyst was filtered after 2 h and washed with deionized water. Nanosized ceria and zirconia, hereafter referred to as nCeO2 and nZrO2, were synthesized according to a previously reported method.30 Briefly, an aqueous solution of Ce(NO3)3*6H2O or ZrO(NO3)2*xH2O (0.8 M, 375 mL) was added to a solution of NH4OH in deionized water (0.8 M, 1.1 L). After stirring for 30 min, the solution was aged at 100 degC for 24 h in a polyethylene vessel. The mixture was cooled down, filtered and washed with an excess amount of deionized water. The resulting particles were dried under vacuum and calcined under an air flow of 100 mL min-1 at 400 degC for 4 h. The other support materials were purchased from Sigma Aldrich and used as received (see ESI+).",
+        "measurement_extractions": [
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "Au catalyst",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "Au catalyst",
+                "measured_property": "reduced"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "225 degC",
+                "unit": "degC",
+                "measured_entity": "Au catalyst",
+                "measured_property": "reduced"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "5%",
+                "unit": "%",
+                "measured_entity": "N2",
+                "measured_property": "H2"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "100 mL min-1",
+                "unit": "mL min-1",
+                "measured_entity": "5% H2 in N2",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "1 L",
+                "unit": "L",
+                "measured_entity": "solution",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "100 \u03bcg mL-1",
+                "unit": "\u03bcg mL-1",
+                "measured_entity": "solution",
+                "measured_property": "HAuCl4*3H2O"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "2.5 g",
+                "unit": "g",
+                "measured_entity": "2 wt% solution of poly(vinyl alcohol) (PVA",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "2 wt%",
+                "unit": "wt%",
+                "measured_entity": "solution",
+                "measured_property": "poly(vinyl alcohol) (PVA"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "MW ~ 10000",
+                "unit": "MW",
+                "measured_entity": "poly(vinyl alcohol) (PVA",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "2 h",
+                "unit": "h",
+                "measured_entity": "Au/AC catalyst",
+                "measured_property": "filtered"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "solution",
+                "measured_property": "stirring"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "100 degC",
+                "unit": "degC",
+                "measured_entity": "solution",
+                "measured_property": "aged"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "solution",
+                "measured_property": "aged"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "2 g",
+                "unit": "g",
+                "measured_entity": "metal oxide",
+                "measured_property": "suspension"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "25 mL",
+                "unit": "mL",
+                "measured_entity": "water",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "0.1 M",
+                "unit": "M",
+                "measured_entity": "NaBH4",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "20 mL",
+                "unit": "mL",
+                "measured_entity": "NaBH4",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "175 mg",
+                "unit": "mg",
+                "measured_entity": "solution",
+                "measured_property": "HAuCl4*3H2O"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "80 mL",
+                "unit": "mL",
+                "measured_entity": "solution",
+                "measured_property": "deionized water"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "10",
+                "unit": null,
+                "measured_entity": "solution",
+                "measured_property": "pH"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "0.2 M",
+                "unit": "M",
+                "measured_entity": "NaOH solution",
+                "measured_property": "adding"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "18 h",
+                "unit": "h",
+                "measured_entity": "stirring",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "100 mesh",
+                "unit": "mesh",
+                "measured_entity": "activated carbon (Darco(r)",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "2 g",
+                "unit": "g",
+                "measured_entity": "support",
+                "measured_property": "adding"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "0.8 M",
+                "unit": "M",
+                "measured_entity": "aqueous solution of Ce(NO3)3*6H2O or ZrO(NO3)2*xH2O",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "375 mL",
+                "unit": "mL",
+                "measured_entity": "aqueous solution of Ce(NO3)3*6H2O or ZrO(NO3)2*xH2O",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "0.8 M",
+                "unit": "M",
+                "measured_entity": "solution of NH4OH in deionized water",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "1.1 L",
+                "unit": "L",
+                "measured_entity": "solution of NH4OH in deionized water",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "100 mL min-1",
+                "unit": "mL min-1",
+                "measured_entity": "calcined",
+                "measured_property": "air flow"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "400 degC",
+                "unit": "degC",
+                "measured_entity": "air flow",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101039c3gc41362d",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "resulting particles",
+                "measured_property": "calcined"
+            }
+        ],
+        "split": "test",
+        "docId": "101039c3gc41362d",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1039/c5ta01668a\nHysteresis-free and highly stable perovskite solar cells produced via a chlorine-mediated interdiffusion method\nAll chemicals were purchased from commercial suppliers and used as received unless stated otherwise. PbI2 (Sigma Aldrich, 99%) and methyl ammonium iodide (MAI) (Wako Chem., 98%) were dissolved in anhydrous N,N-dimethylformamide (Wako chem., 99.5%) (50 mg ml-1), respectively. For chlorine doping, 5-20 wt% MACl (Wako chem.) was mixed with the MAI solution. PC61BM (Solenne or Lumitec, 99%) solution (2 wt%) dissolved in anhydrous chlorobenzene (Wako chem., 99%) was used for coating of the electron selective layer. All the solutions were filtered using 0.45 \u03bcm syringe filters to avoid the risk of particle formation. UV-curable resins (NagaseChemtex XNR5516Z) were used to seal devices with cavity glasses. The X-ray diffraction patterns of MAPbI3 and MAPbI3-xClx were collected using Bruker D8 advanced X-ray diffractometer (CuK\u03b1 radiation, \u03bb = 1.54050 \u00c5). The top surface and cross-sectional images were taken by a high resolution scanning electron microscope at 5 kV accelerating voltage (Hitachi-4800). Additionally, elemental mapping was done using energy dispersive X-ray measurement mode at accelerating voltage of 10 kV. S9+) and incident monochromatic photon to current conversion efficiency (IPCE) spectra or External quantum efficiency (EQE) were measured with a CEP-200BX spectrometer (Bunkokeiki, Tokyo, Japan) at room temperature. Histogram of over 240 devices were generated from the devices using 0.18 cm2 aperture mask.",
+        "measurement_extractions": [
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "99%",
+                "unit": "%",
+                "measured_entity": "PC61BM",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "2 wt%",
+                "unit": "wt%",
+                "measured_entity": "solution",
+                "measured_property": "PC61BM"
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "99%",
+                "unit": "%",
+                "measured_entity": "anhydrous chlorobenzene",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "5 kV",
+                "unit": "kV",
+                "measured_entity": "high resolution scanning electron microscope",
+                "measured_property": "accelerating voltage"
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "10 kV",
+                "unit": "kV",
+                "measured_entity": "X-ray measurement",
+                "measured_property": "accelerating voltage"
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "99%",
+                "unit": "%",
+                "measured_entity": "PbI2",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "98%",
+                "unit": "%",
+                "measured_entity": "methyl ammonium iodide (MAI)",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "99.5%",
+                "unit": "%",
+                "measured_entity": "anhydrous N,N-dimethylformamide",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "50 mg ml-1",
+                "unit": "mg ml-1",
+                "measured_entity": null,
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "5-20 wt%",
+                "unit": "wt%",
+                "measured_entity": "MACl",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "0.45 \u03bcm",
+                "unit": "\u03bcm",
+                "measured_entity": "syringe filters",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "1.54050 \u00c5",
+                "unit": "\u00c5",
+                "measured_entity": "Bruker D8 advanced X-ray diffractometer (CuK\u03b1 radiation",
+                "measured_property": "\u03bb"
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "0.18 cm2",
+                "unit": "cm2",
+                "measured_entity": "aperture mask",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta01668a",
+                "quantity": "over 240",
+                "unit": null,
+                "measured_entity": "Histogram",
+                "measured_property": "devices"
+            }
+        ],
+        "split": "test",
+        "docId": "101039c5ta01668a",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "The elements, Ba (rod, 99+%), Se (shots, 99.999%) and Cr (powder -325 Mesh, 99%) all from Alfa Aesar, were used as received. The synthesis of the solid-solution samples was performed following ref. 20. BaSe was prepared by mechanical alloying using appropriate amounts of the elements (10 g total) loaded in 20 ml tungsten carbide jars and using 7 balls of the same material. The mechanical alloying synthesis was achieved using a Fritsch Pulverisette 7 PL, with a program of 15 cycles of 2 minutes at a speed of 700 rpm. BaxCr5Se8 was then prepared from an appropriate amount of BaSe and elemental Cr and Se. In order to obtain 5 g of the title phase, precursors were ground, mixed and placed in an alumina boat in a sealed silica tube, and heated to 873 K in 10 hours, the temperature at which it remained for two days. The mixture was then slowly cooled to room temperature within 10 hours and a homogeneous dark grey powder was obtained. The powder was compacted using spark plasma sintering (FCT HP D 25/1) in order to produce dense samples for physical property measurements. About 5 g of the sample were inserted into high density graphite dies (Carbonloraine) with an inner diameter of 15 mm. The temperature was raised in 45 minutes to 973 K, this temperature plateau lasted 40 minutes before a 45 minutes ramp down to room temperature. The pressure was raised from 28 MPa to 50 MPa during the heating step, kept constant over the temperature plateau and released during the cooling step.",
+        "measurement_extractions": [
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "10 g",
+                "unit": "g",
+                "measured_entity": "elements",
+                "measured_property": "loaded"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "20 ml",
+                "unit": "ml",
+                "measured_entity": "tungsten carbide jars",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "7 balls",
+                "unit": "balls",
+                "measured_entity": "same material",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "99+%",
+                "unit": "%",
+                "measured_entity": "Ba",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "99.999%",
+                "unit": "%",
+                "measured_entity": "Se",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "99%",
+                "unit": "%",
+                "measured_entity": "Cr",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "-325 Mesh",
+                "unit": "Mesh",
+                "measured_entity": null,
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "5 g",
+                "unit": "g",
+                "measured_entity": "sample",
+                "measured_property": "inserted"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "15 mm",
+                "unit": "mm",
+                "measured_entity": "high density graphite dies",
+                "measured_property": "inner diameter"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "5 g",
+                "unit": "g",
+                "measured_entity": "title phase",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "873 K",
+                "unit": "K",
+                "measured_entity": "precursors",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "10 hours",
+                "unit": "hours",
+                "measured_entity": "precursors",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "10 hours",
+                "unit": "hours",
+                "measured_entity": "mixture",
+                "measured_property": "slowly cooled"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "15 cycles",
+                "unit": "cycles",
+                "measured_entity": "mechanical alloying synthesis",
+                "measured_property": "program"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "2 minutes",
+                "unit": "minutes",
+                "measured_entity": "mechanical alloying synthesis",
+                "measured_property": "program"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "700 rpm",
+                "unit": "rpm",
+                "measured_entity": "mechanical alloying synthesis",
+                "measured_property": "speed"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "45 minutes",
+                "unit": "minutes",
+                "measured_entity": "temperature",
+                "measured_property": "raised"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "973 K",
+                "unit": "K",
+                "measured_entity": "temperature",
+                "measured_property": "raised"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "40 minutes",
+                "unit": "minutes",
+                "measured_entity": "temperature",
+                "measured_property": "plateau"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "45 minutes",
+                "unit": "minutes",
+                "measured_entity": "temperature",
+                "measured_property": "ramp down"
+            },
+            {
+                "docId": "101039c6dt02166b",
+                "quantity": "from 28 MPa to 50 MPa",
+                "unit": "MPa",
+                "measured_entity": "pressure",
+                "measured_property": "raised"
+            }
+        ],
+        "split": "test",
+        "docId": "101039c6dt02166b",
+        "dataset": "msp"
+    }
+]

msp_paragraph_level_no_spans_val.json

@@ -0,0 +1,1502 @@
+[
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "Mg 2 Si 0.45 Sn 0.55 Based Thermoelectric Solid Solutions with Band Convergence\n\nMg2(1+x)Si0.45Sn0.537Sb0.013 (x = 0.04, 0.06, 0.08, 0.10, 0.12) compounds were synthesized by a B2O3 flux method.22 Elemental Mg (99%), Si (99.9%), Sn (99.5%) and Sb (99.999%) powders were utilized. All preparation steps were performed in an argon glove box. Raw powders were weighed, and thoroughly mixed in an agate mortar. The starting materials were transferred into an alumina crucible, covered by B2O3 powders and then compacted. The crucibles were placed into a chamber furnace, heated at 973 K for 10 h and finally cooled down to room temperature. The ingots were ground and sieved to ~50 \u03bcm and hot pressed in a graphite die of \u03a6 12.7 mm under a pressure of 80 MPa at 1025 K for 2 h, resulting in compact pellets for property analysis.",
+        "measurement_extractions": [
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "99.9%",
+                "unit": "%",
+                "measured_entity": "Si",
+                "measured_property": null
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "99.5%",
+                "unit": "%",
+                "measured_entity": "Sn",
+                "measured_property": null
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "99.999%",
+                "unit": "%",
+                "measured_entity": "Sb",
+                "measured_property": null
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "50 \u03bcm",
+                "unit": "\u03bcm",
+                "measured_entity": "ingots",
+                "measured_property": "ground and sieved"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "12.7 mm",
+                "unit": "mm",
+                "measured_entity": "graphite die",
+                "measured_property": "hot pressed"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "80 MPa",
+                "unit": "MPa",
+                "measured_entity": "ingots were ground and sieved",
+                "measured_property": "pressure"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "1025 K",
+                "unit": "K",
+                "measured_entity": "ingots were ground and sieved",
+                "measured_property": "hot pressed"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "2 h",
+                "unit": "h",
+                "measured_entity": "ingots were ground and sieved",
+                "measured_property": "hot pressed"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "0.04",
+                "unit": null,
+                "measured_entity": "Mg2(1+x)Si0.45Sn0.537Sb0.013",
+                "measured_property": "x"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "0.06",
+                "unit": null,
+                "measured_entity": "Mg2(1+x)Si0.45Sn0.537Sb0.013",
+                "measured_property": "x"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "0.08",
+                "unit": null,
+                "measured_entity": "Mg2(1+x)Si0.45Sn0.537Sb0.013",
+                "measured_property": "x"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "0.10",
+                "unit": null,
+                "measured_entity": "Mg2(1+x)Si0.45Sn0.537Sb0.013",
+                "measured_property": "x"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "0.12",
+                "unit": null,
+                "measured_entity": "Mg2(1+x)Si0.45Sn0.537Sb0.013",
+                "measured_property": "x"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "99%",
+                "unit": "%",
+                "measured_entity": "Elemental Mg",
+                "measured_property": null
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "973 K",
+                "unit": "K",
+                "measured_entity": "crucibles",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101002aenm201300174",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "crucibles",
+                "measured_property": "heated"
+            }
+        ],
+        "split": "val",
+        "docId": "101002aenm201300174",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.jallcom.2016.05.264\nMulti-shelled NiO hollow spheres: Easy hydrothermal synthesis and lithium storage performances\n\nSynthesis of multi-shelled NiO hollow spheres: In a typical experiment, 0.01 mol d-glucose and 0.02 mol Ni(NO3)2*6H2O were dissolved in 50 ml utrapure water. Then, the solution was homogenized by vigorous stirring. After stirring for 30 min, the resultant mixture was transferred to a 100 ml Teflon-lined autoclave followed by hydrothermal treatment at 180 degC for 20 h. The obtained products were washed and filtered off several times using utrapure water and ethanol successively, and finally dried in a vacuum oven at 80 degC for 12 h. After synthesis, the products were subjected to annealing at 270, 350, 430 or 550 degC for 3 h in air with a heating rate of 2 degC min-1 from room temperature to obtain multi-shelled NiO hollow spheres with a controlled number of shells (solid NiO sphere, double-, triple- and quadruple/quintuple-shelled NiO hollow sphere, respectively).",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "products",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "products",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "0.01 mol",
+                "unit": "mol",
+                "measured_entity": "d-glucose",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "0.02 mol",
+                "unit": "mol",
+                "measured_entity": "Ni(NO3)2*6H2O",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "50 ml",
+                "unit": "ml",
+                "measured_entity": "utrapure water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "100 ml",
+                "unit": "ml",
+                "measured_entity": "Teflon-lined autoclave",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "180 degC",
+                "unit": "degC",
+                "measured_entity": "resultant mixture",
+                "measured_property": "hydrothermal treatment"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "20 h",
+                "unit": "h",
+                "measured_entity": "resultant mixture",
+                "measured_property": "hydrothermal treatment"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "270, 350, 430 or 550 degC",
+                "unit": "degC",
+                "measured_entity": "products",
+                "measured_property": "annealing"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "2 degC min-1",
+                "unit": "degC min-1",
+                "measured_entity": "products",
+                "measured_property": "heating rate"
+            },
+            {
+                "docId": "101016jjallcom201605264",
+                "quantity": "3 h",
+                "unit": "h",
+                "measured_entity": "products",
+                "measured_property": "annealing"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jjallcom201605264",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.jpowsour.2014.11.037\nPhase composition and electrochemical performance of sodium lithium titanates as anode materials for lithium rechargeable batteries\n\nNaxLi4-xTi6O14 (0 <= x <= 4) samples with different Na contents (x = 0, 1, 2, 3 and 4) were synthesized by a traditional solid-state method. The stoichiometric amounts of CH3COOLi*2H2O (Aladdin Chemistry), CH3COONa*3H2O (Aladdin Chemistry), TiO2 (Aladdin Chemistry) were mixed with oxalic acid dehydrate chelating agent (Aladdin Chemistry) under various Na/Li molar ratios and pretreated by high energy ball-milling in ethanol at 400 rpm rotational speed for 15 h. The obtained precursor slurry was dried at 80 degC and then calcinated at 900 degC for 10 h in air atmosphere.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjpowsour201411037",
+                "quantity": "400 rpm",
+                "unit": "rpm",
+                "measured_entity": "stoichiometric amounts of CH3COOLi*2H2O (Aladdin Chemistry), CH3COONa*3H2O (Aladdin Chemistry), TiO2 (Aladdin Chemistry) were mixed with oxalic acid dehydrate chelating agent",
+                "measured_property": "high energy ball-milling"
+            },
+            {
+                "docId": "101016jjpowsour201411037",
+                "quantity": "15 h",
+                "unit": "h",
+                "measured_entity": "stoichiometric amounts of CH3COOLi*2H2O (Aladdin Chemistry), CH3COONa*3H2O (Aladdin Chemistry), TiO2 (Aladdin Chemistry) were mixed with oxalic acid dehydrate chelating agent",
+                "measured_property": "high energy ball-milling"
+            },
+            {
+                "docId": "101016jjpowsour201411037",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "obtained precursor slurry",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jjpowsour201411037",
+                "quantity": "900 degC",
+                "unit": "degC",
+                "measured_entity": "obtained precursor slurry",
+                "measured_property": "calcinated"
+            },
+            {
+                "docId": "101016jjpowsour201411037",
+                "quantity": "10 h",
+                "unit": "h",
+                "measured_entity": "obtained precursor slurry",
+                "measured_property": "calcinated"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jjpowsour201411037",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.jpowsour.2015.12.048\nSynthesis of sub-10 nm copper sulphide rods as high-performance anode for long-cycle life Li-ion batteries\n\nCopper acetate monohydrate (analytical reagent (AR)), pyridine (AR), and sodium sulfide nonahydrate (AR) were purchased from Sigma-Aldrich. The electrolyte was purchased from Guo Tai Hua Long Company, including 1 M LiPF6 in ethylene carbonate (EC) and dimethyl carbonate (DMC) (1:1 by volume). All chemicals were used without further purification. \n\nIn a typical synthesis, 5.0 mmol of copper acetate monohydrate was dissolved into 40 mL distilled water/pyridine mixture (v:v = 1:3) and heated to 80 degC. 5.0 mmol of sodium sulfide nonahydrate was dissolved into 20 mL of distilled water. Then, sodium sulfide solution was dropped into copper acetate solution under vigorous stirring. Finally, the mixture reacted for 2 h at 80 degC. The final products was collected and washed several times by distilled water or other solvents (e.g., ethanol, pyridine), and then dried in a vacuum at 60 degC for 12 h.\n\n",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "1 M",
+                "unit": "M",
+                "measured_entity": "LiPF6",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "1:1 by volume",
+                "unit": "by volume",
+                "measured_entity": "ethylene carbonate (EC) and dimethyl carbonate (DMC)",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "5.0 mmol",
+                "unit": "mmol",
+                "measured_entity": "copper acetate monohydrate",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "40 mL",
+                "unit": "mL",
+                "measured_entity": "distilled water/pyridine mixture",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "1:3",
+                "unit": null,
+                "measured_entity": "distilled water/pyridine mixture",
+                "measured_property": "v:v"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "5.0 mmol of copper acetate monohydrate was dissolved into 40 mL distilled water/pyridine mixture",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "5.0 mmol",
+                "unit": "mmol",
+                "measured_entity": "sodium sulfide nonahydrate",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "20 mL",
+                "unit": "mL",
+                "measured_entity": "distilled water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "2 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "reacted"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "80 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "reacted"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "final products",
+                "measured_property": "dried in a vacuum"
+            },
+            {
+                "docId": "101016jjpowsour201512048",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "final products",
+                "measured_property": "dried in a vacuum"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jjpowsour201512048",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.jssc.2009.11.025\nCrystal growth, structure and magnetic properties of the double perovskites Ln2MgIrO6 (Ln=Pr, Nd, Sm-Gd)\n\nFor all compounds, the lanthanide sesquioxides, Ln2O3 (Nd, Sm, Eu, Gd), (Alfa Aesar, 99.99%) were fired at 1000 degC for 12 h prior to the reactions. Pr6O11 (Alfa Aesar, 99.9%) was converted to Pr2O3 by heating Pr6O11 at 1000 degC for 24 h under a reducing 5% H2 atmosphere. KOH (Fisher Scientific, A.C.S Reagent Grade, 99.9%), iridium powder (Engelhard, 99.99%) and MgO (Alfa Aesar, 99.998%) were used as received. Single crystals of Ln2MgIrO6 were grown from a high temperature melt of potassium hydroxide. Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes and heated in a box furnace to a temperature of 700 degC at 10 degC/min, held for 24 h at 700 degC, slow cooled to 600 degC at 0.2 degC/min and then allowed to cool to room temperature by turning off the furnace. The black crystals were removed from the flux matrix by dissolving the flux in water aided by sonication. The crystals were finally extracted by vacuum filtration.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "99.9%",
+                "unit": "%",
+                "measured_entity": "Pr6O11",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "1000 degC",
+                "unit": "degC",
+                "measured_entity": "Pr6O11",
+                "measured_property": "heating"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "Pr6O11",
+                "measured_property": "heating"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "5%",
+                "unit": "%",
+                "measured_entity": "atmosphere",
+                "measured_property": "H2"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "Ln2O3",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "1000 degC",
+                "unit": "degC",
+                "measured_entity": "Ln2O3",
+                "measured_property": "fired"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "Ln2O3",
+                "measured_property": "fired"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "99.9%",
+                "unit": "%",
+                "measured_entity": "KOH",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "iridium powder",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "99.998%",
+                "unit": "%",
+                "measured_entity": "MgO",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "700 degC at 10 degC/min, held for 24 h at 700 degC",
+                "unit": "degC",
+                "measured_entity": "Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "0.2 degC/min",
+                "unit": "degC/min",
+                "measured_entity": "Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes",
+                "measured_property": "cooled"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "4 g",
+                "unit": "g",
+                "measured_entity": "KOH",
+                "measured_property": "loaded into sealed silver tubes"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "1 mmol",
+                "unit": "mmol",
+                "measured_entity": "MgO",
+                "measured_property": "loaded into sealed silver tubes"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "10 degC/min",
+                "unit": "degC/min",
+                "measured_entity": "Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "600 degC",
+                "unit": "degC",
+                "measured_entity": "Ln2O3 (Pr, Nd, Sm, Eu, Gd) (0.5 mmol), MgO (1 mmol), Ir (0.5 mmol), and KOH (4 g) were loaded into sealed silver tubes",
+                "measured_property": "cooled"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "0.5 mmol",
+                "unit": "mmol",
+                "measured_entity": "Ir",
+                "measured_property": "loaded into sealed silver tubes"
+            },
+            {
+                "docId": "101016jjssc200911025",
+                "quantity": "0.5 mmol",
+                "unit": "mmol",
+                "measured_entity": "Ln2O3",
+                "measured_property": "loaded into sealed silver tubes"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jjssc200911025",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "In a typical process, 2.5 mmol La(NO3)3*6H2O, 2.24 g 50% Mn(NO3)2 solution (containing 7 mmol Mn2+), 10 mmol citric acid (C6H8O7*H2O), 45 mmol urea and 1.0 g P123 were dissolved with a mixed solvent containing 2 mL ethanol, 8 mL ethylene glycol and 2 mL H2O. After being stirred for 5 h, the obtained solution was transferred into a 70 mL stainless autoclave, and heated at 100 degC for 48 h. The solid product was washed and collected by centrifugation, then dried overnight at 60 degC. This gray product was calcined at 600 degC for 8 h in air flow to convert it to LaMnO3.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "2.5 mmol",
+                "unit": "mmol",
+                "measured_entity": "La(NO3)3*6H2O",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "2.24 g",
+                "unit": "g",
+                "measured_entity": "50% Mn(NO3)2 solution",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "50%",
+                "unit": "%",
+                "measured_entity": "solution",
+                "measured_property": "Mn(NO3)2"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "7 mmol",
+                "unit": "mmol",
+                "measured_entity": "Mn2+",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "10 mmol",
+                "unit": "mmol",
+                "measured_entity": "citric acid (C6H8O7*H2O)",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "45 mmol",
+                "unit": "mmol",
+                "measured_entity": "urea",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "1.0 g",
+                "unit": "g",
+                "measured_entity": "P123",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "2 mL",
+                "unit": "mL",
+                "measured_entity": "solvent",
+                "measured_property": "ethanol"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "8 mL",
+                "unit": "mL",
+                "measured_entity": "solvent",
+                "measured_property": "ethylene glycol"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "2 mL",
+                "unit": "mL",
+                "measured_entity": "solvent",
+                "measured_property": "H2O"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "70 mL",
+                "unit": "mL",
+                "measured_entity": "stainless autoclave",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "100 degC",
+                "unit": "degC",
+                "measured_entity": "obtained solution",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "48 h",
+                "unit": "h",
+                "measured_entity": "obtained solution",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "solid product",
+                "measured_property": "dried overnight"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "600 degC",
+                "unit": "degC",
+                "measured_entity": "gray product",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jmatlet201210091",
+                "quantity": "8 h",
+                "unit": "h",
+                "measured_entity": "gray product",
+                "measured_property": "calcined"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jmatlet201210091",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.matlet.2017.01.142\nTemplate synthesis of Zn2TiO4 and Zn2Ti3O8 nanorods by hydrothermal-calcination combined processes\n0.200 mol Zn(NO3)2*6H2O and 0.015 mol La(NO3)3*6H2O were dissolved in 100 ml de-ionized water. Then 0.100 mol and 0.300 mol C4K2O9Ti*2H2O in 100 ml de-ionized water each were slowly added to the transparency solutions with keeping the pH at 10 throughout the process. These solutions were hydrothermally processed at 120 degC for 12 h. The samples were calcined at 750 degC for 5 h for further characterization.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "0.200 mol",
+                "unit": "mol",
+                "measured_entity": "Zn(NO3)2*6H2O",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "0.015 mol",
+                "unit": "mol",
+                "measured_entity": "La(NO3)3*6H2O",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "100 ml",
+                "unit": "ml",
+                "measured_entity": "de-ionized water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "0.100 mol",
+                "unit": "mol",
+                "measured_entity": "C4K2O9Ti*2H2O",
+                "measured_property": "slowly added"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "0.300 mol",
+                "unit": "mol",
+                "measured_entity": "C4K2O9Ti*2H2O",
+                "measured_property": "slowly added to the transparency solutions"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "10",
+                "unit": null,
+                "measured_entity": "transparency solutions",
+                "measured_property": "pH"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "100 ml",
+                "unit": "ml",
+                "measured_entity": "de-ionized water",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "120 degC",
+                "unit": "degC",
+                "measured_entity": "solutions",
+                "measured_property": "hydrothermally processed"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "solutions",
+                "measured_property": "hydrothermally processed"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "750 degC",
+                "unit": "degC",
+                "measured_entity": "samples",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101016jmatlet201701142",
+                "quantity": "5 h",
+                "unit": "h",
+                "measured_entity": "samples",
+                "measured_property": "calcined"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jmatlet201701142",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.molcata.2014.11.015\nKeggin type heteropoly acid, encapsulated in metal-organic framework: A heterogeneous and recyclable nanocatalyst for selective oxidation of sulfides and deep desulfurization of model fuels\nFor the synthesis of PMo@HKUST-1(I), PW@HKUST-1(II) and SiW@HKUST-1(III) catalysts, the mixture of BTC (0.21 g, 1 mmol) and 0.10 g of CTAB in absolute ethanol (14 mL) was prepared and then 0.06 g of PMo for (I), 0.1 g of PW for (II), 0.1 g of SiW for (III), and 1.45 g of copper(II) nitrate trihydrate (Cu(NO3)2*3H2O) were dissolved in distilled water (10 mL), Both solutions were combined and mixed under vigorous stirring for approximately 30 min and were aged without stirring for a further 2 days in the case of (I) and 4 days for (II and III) at room temperature. A green (I), blue (II) and light blue (III) precipitate were then collected, washed with distilled water three times and dried at 60 degC for 24 h. CTAB was removed by Soxhlet extraction with ethanol (laboratory use, Chem-Lab) which was performed for 24 h. The product was dried in air at 60 degC. The yields were 95%, 92.6% and 86.4% for (I), (II) and (III) respectively.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "2 days in the case of (I) and 4 days",
+                "unit": "days",
+                "measured_entity": "solutions",
+                "measured_property": "aged"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "0.1 g",
+                "unit": "g",
+                "measured_entity": "PW",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "0.21 g",
+                "unit": "g",
+                "measured_entity": "BTC",
+                "measured_property": "mixture"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "14 mL",
+                "unit": "mL",
+                "measured_entity": "absolute ethanol",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "1.45 g",
+                "unit": "g",
+                "measured_entity": "copper(II) nitrate trihydrate (Cu(NO3)2*3H2O)",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "30 min",
+                "unit": "min",
+                "measured_entity": "solutions",
+                "measured_property": "mixed under vigorous stirring"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "1 mmol",
+                "unit": "mmol",
+                "measured_entity": "BTC",
+                "measured_property": "mixture"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "0.1 g",
+                "unit": "g",
+                "measured_entity": "SiW",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "0.06 g",
+                "unit": "g",
+                "measured_entity": "PMo",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "0.10 g",
+                "unit": "g",
+                "measured_entity": "CTAB",
+                "measured_property": "mixture"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "10 mL",
+                "unit": "mL",
+                "measured_entity": "n distilled water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "A green (I), blue (II) and light blue (III) precipitate",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "A green (I), blue (II) and light blue (III) precipitate",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "Soxhlet extraction",
+                "measured_property": "performed"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "product",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "95%",
+                "unit": "%",
+                "measured_entity": "yields",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jmolcata201411015",
+                "quantity": "92.6%",
+                "unit": "%",
+                "measured_entity": "yields",
+                "measured_property": null
+            }
+        ],
+        "split": "val",
+        "docId": "101016jmolcata201411015",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.nanoen.2014.10.008\nFormic acid-reduced ultrasmall Pd nanocrystals on graphene to provide superior electocatalytic activity and stability toward formic acid oxidation\n\nThe graphene oxide (GO) was synthesized from graphite by using a modified Hummers method [20] and [21]. The prepared graphene oxide was dried in normal vacuum at 70 degC for 12 h and then put into a glass bottle under high vacuum level at 60 degC overnight, followed by heating to 220 degC quickly. \n\nIn a typical synthesis of Pd@Graphene electrocatalyst (30% Pd), graphene 10.5 mg, poly(vinyl pyrrolidone) (PVP) 40 mg, and (NH4)2PdCl4 12 mg were dissolved in 2 mL of deionized water. The mixture was treated in an ultrasonic bath to form a uniform aqueous dispersion, then added 3 mL HCOOH and ultrasonically treated for 10 min. The obtained black power was isolated by centrifugation, cleaned by three cycles of centrifugation/washing, and oven-dried at 60 degC for more than 6 h.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "30%",
+                "unit": "%",
+                "measured_entity": "Pd",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "10.5 mg",
+                "unit": "mg",
+                "measured_entity": "graphene",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "40 mg",
+                "unit": "mg",
+                "measured_entity": "poly(vinyl pyrrolidone) (PVP)",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "12 mg",
+                "unit": "mg",
+                "measured_entity": "(NH4)2PdCl4",
+                "measured_property": "dissolved"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "2 mL",
+                "unit": "mL",
+                "measured_entity": "deionized water",
+                "measured_property": null
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "70 degC",
+                "unit": "degC",
+                "measured_entity": "graphene oxide",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "graphene oxide",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "graphene oxide",
+                "measured_property": "high vacuum level"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "220 degC",
+                "unit": "degC",
+                "measured_entity": "graphene oxide",
+                "measured_property": "heating"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "3 mL",
+                "unit": "mL",
+                "measured_entity": "HCOOH",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "10 min",
+                "unit": "min",
+                "measured_entity": "uniform aqueous dispersion, then added 3 mL HCOOH",
+                "measured_property": "ultrasonically treated"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "60 degC",
+                "unit": "degC",
+                "measured_entity": "obtained black power",
+                "measured_property": "oven-dried"
+            },
+            {
+                "docId": "101016jnanoen201410008",
+                "quantity": "more than 6 h",
+                "unit": "h",
+                "measured_entity": "obtained black power",
+                "measured_property": "oven-dried"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jnanoen201410008",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1016/j.solidstatesciences.2016.09.005\nDielectric properties of FeNbO4 ceramics prepared by the sol-gel method\n\nFeNbO4 powders were prepared using the sol-gel method. Niobium chloride (NbCl5) and iron nitrate (Fe(NO3)3*9H2O), were used as starting materials and citric acid and ethylene glycol as chelating agent and reaction medium, respectively. A suspension containing stoichiometric amounts of starting materials was previously prepared in a minor amount of hydrogen peroxide (3% V/V) and dispersed in a mixture of citric acid and ethylene glycol in a molar ratio 1:3. In order to promote the solubility, the suspension was stirred until a clear colloidal suspension was obtained. \n\nThe solution was dried at 300 degC for 24 h to evaporate the solvent and the obtained powders were thermally analysed by differential thermal analysis, performed in a Lynseis Apparatus type L92/095, in the temperature range 20-1200 degC, with a heating rate of 5 degC/min, using Al2O3 as reference. \n\nSubsequently, the dry powders were pressed into pellets, and finally heat-treated, according to the DTA results, at 500, 650, 850, 1000 and 1200 degC, using a dwell time of 4 h, with a heating rate of 5 oC/min.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "20-1200 degC",
+                "unit": "degC",
+                "measured_entity": "powders were thermally analysed",
+                "measured_property": "temperature range"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "5 degC/min",
+                "unit": "degC/min",
+                "measured_entity": "powders",
+                "measured_property": "heating rate"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "300 degC",
+                "unit": "degC",
+                "measured_entity": "solution",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "solution",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "500, 650, 850, 1000 and 1200 degC",
+                "unit": "degC",
+                "measured_entity": "pellets",
+                "measured_property": "heat-treated"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "pellets",
+                "measured_property": "heat-treated"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "5 oC/min",
+                "unit": "oC/min",
+                "measured_entity": "pellets",
+                "measured_property": "heating rate"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "3% V/V",
+                "unit": "% V/V",
+                "measured_entity": "suspension",
+                "measured_property": "hydrogen peroxide"
+            },
+            {
+                "docId": "101016jsolidstatesciences201609005",
+                "quantity": "1:3",
+                "unit": null,
+                "measured_entity": "citric acid and ethylene glycol",
+                "measured_property": "molar ratio"
+            }
+        ],
+        "split": "val",
+        "docId": "101016jsolidstatesciences201609005",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "A series of polycrystalline samples of SrMo1-xNixO4(0.02<=x<=0.08) were prepared through the conventional solid-state reaction method in air. Appropriate proportions of high-purity SrCO3, MoO3, and Ni powders were thoroughly mixed according to the desired stoichiometry, and then prefired at 900 [ ?]C for 24 h. ?]C for 24 h with intermediate grinding twice. White compounds, SrMo1-xNixO4, were obtained. The compounds were ground and pressed into small pellets about 10 mm diameter and 2 mm thickness.",
+        "measurement_extractions": [
+            {
+                "docId": "101016jssc200704044",
+                "quantity": "10 mm",
+                "unit": "mm",
+                "measured_entity": "pellets",
+                "measured_property": "diameter"
+            },
+            {
+                "docId": "101016jssc200704044",
+                "quantity": "2 mm",
+                "unit": "mm",
+                "measured_entity": "pellets",
+                "measured_property": "thickness"
+            },
+            {
+                "docId": "101016jssc200704044",
+                "quantity": "900",
+                "unit": null,
+                "measured_entity": "high-purity SrCO3, MoO3, and Ni powders",
+                "measured_property": "prefired"
+            },
+            {
+                "docId": "101016jssc200704044",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": null,
+                "measured_property": null
+            },
+            {
+                "docId": "101016jssc200704044",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": null,
+                "measured_property": null
+            }
+        ],
+        "split": "val",
+        "docId": "101016jssc200704044",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "Stoichiometric amounts of Ln(NO3)3*6H2O(Aldrich, 99.9%, metal basis), Ba(NO3)2 (Aldrich, 99+%), Sr(NO3)2 (Aldrich, 99+%), Co(NO3)2*6H2O (Aldrich, 98+%), and Fe(NO3)3*6H2O (Aldrich, 98%) were dissolved in distilled water with proper amount of glycine. The solutions were heated up to 350degC in air and followed by combustion to form fine powders, which were calcined at 600degC for 4 hours. The resulting powders were then grinded and calcined again at 900degC for 4 hours.",
+        "measurement_extractions": [
+            {
+                "docId": "101038srep02426",
+                "quantity": "99+%",
+                "unit": "%",
+                "measured_entity": "Sr(NO3)2",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "98+%",
+                "unit": "%",
+                "measured_entity": "Co(NO3)2*6H2O",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "98%",
+                "unit": "%",
+                "measured_entity": "Fe(NO3)3*6H2O",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "99.9%",
+                "unit": "%",
+                "measured_entity": "Ln(NO3)3*6H2O",
+                "measured_property": null
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "up to 350degC",
+                "unit": "degC",
+                "measured_entity": "solutions",
+                "measured_property": "heated"
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "600degC",
+                "unit": "degC",
+                "measured_entity": "fine powders",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "4 hours",
+                "unit": "hours",
+                "measured_entity": "fine powders",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "900degC",
+                "unit": "degC",
+                "measured_entity": "resulting powders",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101038srep02426",
+                "quantity": "4 hours",
+                "unit": "hours",
+                "measured_entity": "resulting powders",
+                "measured_property": "calcined"
+            }
+        ],
+        "split": "val",
+        "docId": "101038srep02426",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1039/c4cy00360h\nCatalytic consequences of micropore topology, mesoporosity, and acidity on the hydrolysis of sucrose over zeolite catalysts\nThe conventional microporous FER, MFI, MOR, BEA, and FAU with different acidity (Si/Al ratio) were purchased from Zeolyst. MWW and PMWW were derived from the same precursor, MWW (P). The hydrothermal synthesis of MWW (P) was carried out by using the method described by Corma et al.39,40 One portion of the crystalline product MWW (P) was dried and calcined to produce MWW. The other portion of MWW (P) was swollen according to the method developed by Maheshwari et al.,41 followed by pillaring of the swollen materials using the procedure reported by Barth et al.38 The resulting solid was treated using the same conditions as those for MWW to produce PMWW. A multilamellar MFI was synthesized using the method reported by Ryoo and co-workers,43 through a coherent assembly of the zeolite layer and the structure directing agent, a diquaternary ammonium surfactant with a relatively long hydrocarbon chain. Pillaring of multilamellar MFI was done as reported by Na et al.42 to produce PMFI, using a similar pillaring procedure to that of swollen MWW (P). The as-synthesized MWW and MFI zeolites were ion-exchanged four times using 1 mol L-1 aqueous NH4NO3 (weight ratio of zeolite to NH4NO3 solution = 1:10) at 353 K for 12 h and subsequently collected by vacuum filtration, washed with deionized (DI) water three times, and dried at 343 K overnight. No ion-exchange process was applied to the commercial zeolites since they were purchased in the NH4+-form. All zeolite samples in their NH4+-form were treated in dry air (100 mL min-1, ultrapure, Airgas) by increasing the temperature from ambient temperature to 823 K at 1.45 K min-1 and holding for 4 h to thermally decompose NH4+ to NH3 and H+. To differentiate the same type of zeolite with different Si/Al ratios, each catalyst is named by its structure type and Si/Al ratio in the remainder of this paper.",
+        "measurement_extractions": [
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "100 mL min-1",
+                "unit": "mL min-1",
+                "measured_entity": "zeolite samples in their NH4+-form",
+                "measured_property": "treated"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "823 K",
+                "unit": "K",
+                "measured_entity": "zeolite samples in their NH4+-form",
+                "measured_property": "temperature"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "1.45 K min-1",
+                "unit": "K min-1",
+                "measured_entity": "zeolite samples in their NH4+-form",
+                "measured_property": "increasing the temperature"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "zeolite samples in their NH4+-form",
+                "measured_property": "holding"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "1 mol L-1",
+                "unit": "mol L-1",
+                "measured_entity": "aqueous NH4NO3",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "1:10",
+                "unit": null,
+                "measured_entity": "zeolite to NH4NO3 solution",
+                "measured_property": "weight ratio"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "353 K",
+                "unit": "K",
+                "measured_entity": "as-synthesized MWW and MFI zeolites",
+                "measured_property": "ion-exchanged"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "as-synthesized MWW and MFI zeolites",
+                "measured_property": "ion-exchanged"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "343 K",
+                "unit": "K",
+                "measured_entity": "as-synthesized MWW and MFI zeolites",
+                "measured_property": "dried"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "four times",
+                "unit": "times",
+                "measured_entity": "as-synthesized MWW and MFI zeolites",
+                "measured_property": "ion-exchanged"
+            },
+            {
+                "docId": "101039c4cy00360h",
+                "quantity": "three times",
+                "unit": "times",
+                "measured_entity": "deionized (DI) water",
+                "measured_property": null
+            }
+        ],
+        "split": "val",
+        "docId": "101039c4cy00360h",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "PrBa 0.8 Ca 0.2 Mn 2 O 5+\u03b4\nIn order to fabricate a La0.9Sr0.1Ga0.8Mg0.2O3-\u03b4 (LSGM) electrolyte supported cell, the LSGM powder was prepared by the solid state reaction method and a dense electrolyte substrate was prepared by dry pressing followed by sintering at 1475 degC. Stoichiometric amounts of La2O3 (Sigma 99.99%), SrCO3 (Sigma, 99.99%), Ga2O3 (Sigma, 99.99%), and MgO (Sigma, 99.9%) powders were ball milled in ethanol for 24 h. After drying, the mixture was calcined for 6 h. The thickness of the LSGM electrolyte was adjusted to about 250 \u03bcm by polishing. LDC (La0.4Ce0.6O2-\u03b4) was also prepared by ball milling stoichiometric amounts of La2O3 and CeO2 (Sigma, 99.99%) in ethanol and then calcined for 6 h. For the preparation of the electrode slurry, disordered Pr0.5Ba0.4Ca0.1MnO3 was mixed with an organic binder, V-006. The Pr0.5Ba0.4Ca0.1MnO3 slurry was applied on both sides of the LSGM pellet by the screen printing method, and then fired at 950 degC in air for 4 h.",
+        "measurement_extractions": [
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "CeO2",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "6 h",
+                "unit": "h",
+                "measured_entity": "ball milling stoichiometric amounts of La2O3 and CeO2 (Sigma, 99.99%) in ethanol",
+                "measured_property": "calcined"
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "950 degC",
+                "unit": "degC",
+                "measured_entity": "Pr0.5Ba0.4Ca0.1MnO3 slurry was applied on both sides of the LSGM pellet",
+                "measured_property": "fired"
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "4 h",
+                "unit": "h",
+                "measured_entity": "Pr0.5Ba0.4Ca0.1MnO3 slurry was applied on both sides of the LSGM pellet",
+                "measured_property": "fired"
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "250 \u03bcm",
+                "unit": "\u03bcm",
+                "measured_entity": "LSGM electrolyte",
+                "measured_property": "thickness"
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "1475 degC",
+                "unit": "degC",
+                "measured_entity": "sintering",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "La2O3",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "SrCO3",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "99.99%",
+                "unit": "%",
+                "measured_entity": "Ga2O3",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "99.9%",
+                "unit": "%",
+                "measured_entity": "MgO",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "24 h",
+                "unit": "h",
+                "measured_entity": "Stoichiometric amounts of La2O3 (Sigma 99.99%), SrCO3 (Sigma, 99.99%), Ga2O3 (Sigma, 99.99%), and MgO (Sigma, 99.9%) powders",
+                "measured_property": "ball milled in ethanol"
+            },
+            {
+                "docId": "101039c5ta08878j",
+                "quantity": "6 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "calcined"
+            }
+        ],
+        "split": "val",
+        "docId": "101039c5ta08878j",
+        "dataset": "msp"
+    },
+    {
+        "instruction": "\n    You are an expert at extracting quantity, units and their related context from text. \n    Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n    ",
+        "paragraph": "10.1039/c5tc00196j\nA facile fabrication of large-scale reduced graphene oxide-silver nanoparticle hybrid film as a highly active surface-enhanced Raman scattering substrate\nNatural graphite flake (99.8% purity), silver nitrate (AgNO3, >99%), and sodium citrate tribasic dehydrate (>=99.0% purity) were purchased from Sigma-Aldrich. R6G and MA were obtained from J&K Scientific Ltd (Beijing, China). H2SO4 (95-98 wt%) and KMnO4 (99.5% purity) were purchased from Beijing Chemical Co., Ltd (Beijing, China). H3PO4 (85% purity) and H2O2 (30% aqueous solution) were obtained from Xilong Chemical Co., Ltd. All chemicals used in this work were of analytical reagent grade and obtained from commercial sources and directly used without additional purification. The water used was purified through a Millipore system (~18.2 M\u03a9 cm-1). Carbon-coated Cu grids for transmission electron microscopy (TEM) characterization were purchased from Plano GmbH (Wetzlar, Germany). \nGO was synthesized by the oxidation of natural graphite flakes using a modified Hummers method to produce graphite oxide.31 In detail, 3 g of graphite flakes were mixed with a mixture of concentrated H2SO4/H3PO4 (9:1) under stirring at room temperature; KMnO4 (18 g) was added slowly by stirring, and the mixture was incubated and stirred in the thermostatic water bath for 12 h (50 degC). The mixture was poured slowly onto ice crush (200 mL) and 10% hydrogen peroxide (10 mL) when the temperature was decreased to room temperature. Then the mixture was centrifuged (4000 rpm for 0.5 h), and the remaining solid material was washed in succession with 400 mL of water, 400 mL of 30% hydrochloric acid, and 400 mL of ethanol (2x). The remaining material was filtered and vacuum-dried overnight at room temperature. Finally, 5.8 g of the product was obtained. \nAgNPs were synthesized according to the literature previously reported.32 In a typical synthesis, 100 mL of aqueous AgNO3 (0.5 mmol) was added into a 250 mL flask and heated to boil under punchy stirring in an oil bath. After that, 10 mL aqueous sodium citrate (1%) was added, and the color of the solution reached to yellow after 1 h, which indicates the formation of AgNPs.",
+        "measurement_extractions": [
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "99.8%",
+                "unit": "%",
+                "measured_entity": "Natural graphite flake",
+                "measured_property": "purity"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": ">99%",
+                "unit": "%",
+                "measured_entity": "silver nitrate (AgNO3",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": ">=99.0%",
+                "unit": "%",
+                "measured_entity": "sodium citrate tribasic dehydrate",
+                "measured_property": "purity"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "~18.2 M\u03a9 cm-1",
+                "unit": "M\u03a9 cm-1",
+                "measured_entity": "water",
+                "measured_property": "purified through a Millipore system"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "200 mL",
+                "unit": "mL",
+                "measured_entity": "ice crush",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "10%",
+                "unit": "%",
+                "measured_entity": "hydrogen peroxide",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "10 mL",
+                "unit": "mL",
+                "measured_entity": "hydrogen peroxide",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "85%",
+                "unit": "%",
+                "measured_entity": "H3PO4",
+                "measured_property": "purity"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "30%",
+                "unit": "%",
+                "measured_entity": "H2O2",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "3 g",
+                "unit": "g",
+                "measured_entity": "graphite flakes",
+                "measured_property": "mixed"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "9:1",
+                "unit": null,
+                "measured_entity": "H2SO4/H3PO4",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "18 g",
+                "unit": "g",
+                "measured_entity": "KMnO4",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "12 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "stirred"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "50 degC",
+                "unit": "degC",
+                "measured_entity": "mixture",
+                "measured_property": "stirred"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "5.8 g",
+                "unit": "g",
+                "measured_entity": "product",
+                "measured_property": "obtained"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "100 mL",
+                "unit": "mL",
+                "measured_entity": "AgNO3",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "0.5 mmol",
+                "unit": "mmol",
+                "measured_entity": "AgNO3",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "250 mL",
+                "unit": "mL",
+                "measured_entity": "flask",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "10 mL",
+                "unit": "mL",
+                "measured_entity": "sodium citrate",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "1%",
+                "unit": "%",
+                "measured_entity": "sodium citrate",
+                "measured_property": "added"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "1 h",
+                "unit": "h",
+                "measured_entity": "solution",
+                "measured_property": "reached to yellow"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "95-98 wt%",
+                "unit": "wt%",
+                "measured_entity": "H2SO4",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "99.5%",
+                "unit": "%",
+                "measured_entity": "KMnO4",
+                "measured_property": "purity"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "4000 rpm",
+                "unit": "rpm",
+                "measured_entity": "mixture",
+                "measured_property": "centrifuged"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "0.5 h",
+                "unit": "h",
+                "measured_entity": "mixture",
+                "measured_property": "centrifuged"
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "400 mL",
+                "unit": "mL",
+                "measured_entity": "water",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "400 mL",
+                "unit": "mL",
+                "measured_entity": "30% hydrochloric acid",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "30%",
+                "unit": "%",
+                "measured_entity": "hydrochloric acid",
+                "measured_property": null
+            },
+            {
+                "docId": "101039c5tc00196j",
+                "quantity": "400 mL",
+                "unit": "mL",
+                "measured_entity": "ethanol",
+                "measured_property": null
+            }
+        ],
+        "split": "val",
+        "docId": "101039c5tc00196j",
+        "dataset": "msp"
+    }
+]